How to Cite: Yadav, N. (2022). A Practical Handbook for Pharmaceutical Chemistry (1st ed., pp. 1-117). Noble Science Press. https://doi.org/10.52458/9789391842611.nsp2022.eb.asu
Description
This book on Pharma Marketing Managements is based on the current D. Pharma PCI regulation ER-20. Pharmaceutical chemistry practical divided into eight parts as per new PCI syllabus. Part 1 includes limit tests for quantitative or semi-quantitative estimation of impurities like chloride, sulphate, Iron and heavy metals in pharmaceuticals. Part 2 includes identification tests for anions and cations as per I.P. in pharmaceuticals. Part 3 includes fundamentals of volumetric analysis for preparation and standardization of secondary standard substances. Part 4 includes assay of various chemical substances and pharmaceuticals using various titration methods like acid-base titration, non-aqueous titration, precipitation titration, complexometric titration and redox titration as per I.P. Part 5 includes fundamentals of preparative organic chemistry for identification of pharmaceutical using melting and boiling point determination. Part 6 includes preparation of pharmaceutically important intermediate such as benzoic acid and picric acid. Part 7 includes identification and test for purity of pharmaceuticals like paracetamol and aspirin. Part 8 includes systematic qualitative analysis of pharmaceuticals and its intermediates as per I.P.
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S. No. |
Title, Authors |
Page no. |
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Part 1: Limit Tests for Impurities |
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1 |
TO PERFORM AND REPORT THE LIMIT TEST FOR CHLORIDE IN THE GIVEN SAMPLE OF SODIUM BICARBONATE AS PER INDIAN PHARMACOPOEIA Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
1-5 |
|
2 |
PERFORM AND REPORT THE LIMIT TEST FOR SULPHATE IN THE GIVEN SAMPLE OF SODIUM BICARBONATE AS PER INDIAN PHARMACOPOEIA Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
6-9 |
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3 |
TO PERFORM AND REPORT THE LIMIT TEST FOR CHLORIDE IN THE GIVEN SAMPLE OF SODIUM CHLORIDE AS PER INDIAN PHARMACOPOEIA
Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
10-13 |
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4 |
TO PERFORM AND REPORT THE LIMIT TEST FOR HEAVY METAL IN THE GIVEN SAMPLE OF SODIUM CHLORIDE AS PER INDIAN PHARMACOPOEIA Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
14-17 |
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Part 2: Identification Tests for Anions and Cations as per I.P. |
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5 |
TO PERFORM AND REPORT IDENTIFICATION TESTS ON GIVEN SAMPLE OF SODIUM CHLORIDE AS PER I.P. Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
18-24 |
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6 |
TO PERFORM AND REPORT IDENTIFICATION TESTS ON GIVEN SAMPLE OF SODIUM BICARBONATE AS PER I.P. Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
25-29 |
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Part 3: Fundamentals of Volumetric Analysis |
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7 |
PREPARATION OF STANDARD SOLUTION AND STANDARDIZATION OF SODIUM HYDROXIDE Dr. Mukesh Kumar Kumawat Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
30-37 |
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8 |
PREPARATION OF STANDARD SOLUTION AND STANDARDIZATION OF POTASSIUM PERMANGANATE Dr. Mukesh Kumar Kumawat Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Mr. Sumit Tewatia Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
38-43 |
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Part 4: Assay of Pharmaceuticals |
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9 |
TO PERFORM ASSAY OF FERROUS SULPHATE (REDOX TITRATION) BY CERIMETRY AND STANDARDIZATION OF TITRANT Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
44-49 |
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10 |
TO PERFORM ASSAY OF ASPIRIN (ACID-BASE TITRATION) AND STANDARDIZATION OF TITRANT Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Mr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
50-57 |
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11 |
TO PERFORM ASSAY OF IBUPROFEN TABLET (ACID-BASE TITRATION) AND STANDARDIZATION OF TITRANT Dr. Mukesh Kumar Kumawat Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
58-62 |
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12 |
TO PERFORM ASSAY OF CALCIUM GLUCONATE TABLET (ACID-BASE TITRATION) AND STANDARDIZATION OF TITRANT Dr. Mohini Kalra Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Mr. Sumit Tewatia Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
63-66 |
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Part 5: Fundamentals of Preparative Organic Chemistry |
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13 |
DETERMINATION OF MELTING POINT OF GIVEN ORGANIC COMPOUNDS Dr. Mohini Kalra Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Anupama Diwan Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
67-73 |
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14 |
DETERMINATION OF BOILING POINT OF GIVEN ORGANIC COMPOUNDS Dr. Mohini Kalra Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Mr. Sumit Tewatia Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
74-78 |
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Part 6: Preparation of Organic Compounds |
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15 |
PREPARATION OF BENZOIC ACID FROM BENZAMIDE Dr. Gufran Ajmal Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
79-84 |
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16 |
PREPARATION OF PICRIC ACID FROM PHENOL Dr. Gufran Ajmal Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
85-89 |
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Part 7: Identification and Test for Purity of Pharmaceuticals |
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17 |
IDENTIFICATION AND TEST FOR PURITY OF ASPIRIN Dr. Gufran Ajmal Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
90-95 |
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18 |
IDENTIFICATION AND TEST FOR PURITY OF PARACETAMOL Mr. Sumit Tewatia Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
96-100 |
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Part 8: Systematic Qualitative Analysis Experiments |
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19 |
TO IDENTIFY THE GIVEN ORGANIC COMPOUND-1 (UREA) BY SYSTEMATIC QUALITATIVE ANALYSIS
Mr. Sumit Tewatia Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
101-109 |
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20 |
TO IDENTIFY THE GIVEN ORGANIC COMPOUND-2 (ETHANOL) BY SYSTEMATIC QUALITATIVE ANALYSIS
Dr. Narender Yadav Assistant Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram Dr. Kapil Kumar Associate Professor, School of Pharmaceutical Sciences, Apeejay Stya University, Gurugram |
110-117 |
Dr. Narender Yadav
Dr. Narender Yadav is working as an Assistant Professor in the Department of Pharmaceutical Chemistry at the School of Pharmaceutical Sciences, Apeejay Stya University. He has done MS (Pharm.) and PhD in Medicinal Chemistry from National Institute of Pharmaceutical Education and Research (NIPER), SAS Nagar. He has 1.5 years of experience in Intellectual Property Right (IPR) at Stellarix Consultancy Services, Jaipur. He has more than 6 years of research experience in Synthetic Organic Chemistry and Carbohydrate Chemistry. His primary areas of research include Sugar & Peptide Derived Bioactive Molecules, Approaches for Sustainable & Green Chemistry, Design & Synthesis of Anti-microbial Agents, Hydroxy Fatty Acid & Its Pharmaceutical Importance, Intellectual Property Right (IPR). He has published several research papers in peer reviewed journals like Carbohydrate Research, RSC Advances and Trends in Carbohydrate Research.
